30 articles for “TD-NMR”

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Research ArticleOpen accessEvery word in the titleMetabolite Profiles of Arsenic Tolerant Plants Regenerated from Stem Calli of Andrographis paniculata (Burm.f.) Nees using HPLC and 1D 1H NMRJ. Vijayakumar, P. Ponmanickam, P. Samuel et al.In vitro culture provide a suitable condition for regeneration of arsenic tolerant plants from stem calli of Andrographis paniculata (Burm.f.) Nees. The regenerated plants could be valuable material applicable to soil remediation. In vitro culture of stem explants on MS basal salts, 3.0% sucrose, 0.8% agar medium fortified with various concentrations of As2O3 (0.0-9.0 µM) along with NAA (3.5 mg … …American Journal of Biochemistry and Biotechnology, Vol. 13, Issue 4 · 27 Oct 2017 · 7,865 accessesView PDF Cite

Research ArticleOpen accessEvery word in the titleThe Investigation of 1H NMR Spectra of 2,3-Dihydro-4-Pyridinones Derived from BisdemethoxycurcuminWisam A. Radhi, Bahjat A. SaeedProblem statement: The studied dihydropyridones were synthesized via microwave assisted reaction of bisdemethoxycurcumin and amines or amine acetates which is new approach in the synthesis of this important class of compounds and the deep study of their NMR spectra seems reasonable. Approach: 1H NMR spectra of dihydropyridones derived from curcumin were discussed and their structures were elucidated accordingly. Results: The … …American Journal of Applied Sciences, Vol. 7, Issue 8 · 31 Aug 2010 · 7,186 accessesView PDF Cite

Research ArticleOpen accessIn the keywordsOil and Fatty Acids in Seed of Eggplant (Solanum melongena L.) and Some Related and Unrelated Solanum SpeciesRobert Jarret, Irvin Levy, Thomas Potter, Steven CermakThe seed oil content of 305 genebank accessions of eggplant (Solanum melongena), five related species (S. aethiopicum L., S. incanum L., S. anguivi Lam., S. linnaeanum Hepper and P.M.L. Jaeger and S. macrocarpon L.) and 27 additional Solanums pecies, was determined by NMR. Eggplant (S. melongena) seed oil content varied from 17.2% (PI 63911317471) to 28.0% (GRIF 13962) with a … …American Journal of Agricultural and Biological Sciences, Vol. 11, Issue 2 · 4 May 2016 · 8,497 accessesView PDF Cite

Research ArticleOpen accessIn the keywordsSynthesis and Characterization of Organotin(IV) N-Benzyl-N-Isopropyldithiocarbamate Compounds: Cytotoxic Assay on Human Hepatocarcinoma Cells (HepG2)Normah Awang, Ibrahim Baba, Nor Syaidatul Akmal Mohd Yousof, Nurul Farahana KamaludinProblem statement: Several studies on organotin(IV) dithiocarbamate compounds have been carried out but not on the synthesis and characterization together with cytotoxic assay of organotin(IV) N-benzyl-N-isopropyldithiocarbamate compounds. Approach: Three new organotin(IV) compounds of type N-benzyl-N-isopropyldithiocarbamate have been successfully synthesized by direct reaction between secondary amine with organotin(IV) chloride using in situ method. All the compounds were characterized using elemental analysis, … …American Journal of Applied Sciences, Vol. 7, Issue 8 · 31 Aug 2010 · 8,092 accessesView PDF Cite

Research ArticleOpen accessIn the keywordsSeparation of Coenzyme Q10 in Palm Oil by Supercritical Fluid ChromatographyNg Mei Han, Choo Yuen May, Ma Ah Ngan et al.Palm oil is known to host a variety of phytonutrients; some having antioxidant property such as the carotenes and vitamin E. These antioxidants are also present in the oil recovered from the palm-pressed fibre. Study was carried out to investigate the presence of coenzyme Q10, yet another non-glyceride compound which possesses antioxidant property in crude palm oil (CPO) and palm … …American Journal of Applied Sciences, Vol. 3, Issue 7 · 31 Jul 2006 · 7,667 accessesView PDF Cite

Research ArticleOpen accessIn the keywordsStability of Neodymium(III) Complexes of 4-Hydroxycoumarins with Anticoagulant ActivityIrena Kostova, Irina NikolovaComplexes of neodymium(III) with 4-hydroxy-3-(3-oxo-1-phenylbutyl)-2H-1-benzopyran-2-one, 4-hydroxy-3-[1-(4-chlorophenyl)-3-oxobutyl]-2H-1-benzopyran-2-one and 4-hydroxy-3-[1-(4-nitrophenyl)-3-oxobutyl]-2H-1-benzopyran-2-one were synthesized by mixing of water solutions of neodymium(III) nitrate and the respective ligands, in amounts equal to metal: ligand molar ratio of 1: 3. The complexes were characterized and identified by elemental analysis, conductivity, IR and 1H NMR spectral data. DTA and TGA have been applied to confirm the compositions of … …American Journal of Pharmacology and Toxicology, Vol. 1, Issue 2 · 30 Jun 2006 · 7,554 accessesView PDF Cite

Research ArticleOpen accessIn the keywordsFactor Analysis, Target Factor Testing and Model Designing of Aromatic Solvent Effect of the Formyl Proton Nuclear Magnetic Resonance Chemical Shift in Para substituted BenzaldehydesGhazwan F. FadhilProblem statement: The variations of formyl proton Chemical Shifts (CS) of p-substituted benzaldehydes in aromatic solvents were investigated. The validity of several physical solvent and empirical solvent scales was examined. Also, to predict dipolarity-polarizability (π*) solvent scale for some aromatic solvents. Model designing was also achieved to rationalize the aromatic solvent effect on the formyl proton CS. Approach: The previously … …American Journal of Applied Sciences, Vol. 7, Issue 1 · 31 Jan 2010 · 7,582 accessesView PDF Cite

Research ArticleOpen accessIn the abstractGastroprotective Effects of β-sitosterol and β-sitosterol-3-O-β-D-glucopyranoside from Bridelia ferruginea Stem BarkEjike Marcellus Nnamani, Peter Achunike Akah, Charles Ogbonnaya Okoli et al.The methanol extract of Bridelia ferruginea Benth. (Euphorbiaceae) stem bark (BFME) was partitioned in chloroform-methanol-water (2:2:1) mixture to obtain the Chloroform (CF) and Aqueous Methanol (AMF) fractions. The BFME, CF and AMF were screened for antiulcer activity using indomethacin-induced ulcer as activity guide. The CF provided the highest gastroprotection and was subsequently fractionated in a silica gel (60-200 mesh) column … …American Journal of Pharmacology and Toxicology, Vol. 15, Issue 1 · 4 Jan 2021 · 7,784 accessesView PDF Cite

Research ArticleOpen accessIn the abstractβ-Naphthalene Incorporated Thiazole-5-Carboxamides/Thiazole -5- Ketones: Design, Synthesis and Anticonvulsant Screening against Two Seizure ModelsMohammed Faiz Arshad, Faisal Al-Otaibi, Gulam Mustafa et al.A bunch of β-naphthalene incorporated thiazole-5-carboxamides/thiazole -5- ketones (7a-7o& 8a-8e) were prepared by reacting 4-methyl-2-(naphthalen-2-yl)thiazole-5-carbonyl chloride with appropriate amines. Structures of all the compounds were explained by elemental analysis, FT-IR, 1H NMR and mass spectral data. The compounds were evaluated for their anticonvulsant activity employing MES and chemoshock (scPTZ) seizure tests. Neurotoxicity was also assessed. Majority of these compounds exhibited … …American Journal of Pharmacology and Toxicology, Vol. 14, Issue 1 · 29 Aug 2019 · 7,494 accessesView PDF Cite

Research ArticleOpen accessIn the abstractNovel Production of Two New Nonpolyenic Antifungal Macrolide Derivatives by Streptomyces Z26 Isolated from Moroccan Rhizospheric SoilAhmed Nafis, Brahim Oubaha, Najoua Elhidar et al.The aim of our study was to screen Moroccan actinomycete isolates able to produce nonpolyenic antifungal metabolites in order to contribute to limiting the problem of fungal infections emergence in particular mycotic diseases and to discover known antifungal families, especially nonpolyenic drugs. 480 isolates were tested against 5clinically pathogenic Candida species. Several methods have been used to study the polyenic … …OnLine Journal of Biological Sciences, Vol. 18, Issue 2 · 8 Mar 2018 · 8,459 accessesView PDF Cite