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53 results for “Mass Spectrometry”

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Research ArticleOpen accessPhrase in the titleMass Spectrometry/Mass Spectrometry Study on the Degradation of B-Aflatoxins in Maize with Aqueous Citric AcidA. Méndez-Albores, I. Nicolás-Vázquez, R. Miranda-Ruvalcaba, E. Moreno-MartÍnezDegradation of B-aflatoxins in maize by means of 1N aqueous citric acid was confirmed by the AFLATEST immunoaffinity column method, High Performance Liquid Chromatography (HPLC), tandem mass spectrometry (MS/MS) and computational information. The AFLATEST and HPLC assays showed that 96.7% degradation occurred in maize contaminated with 93 ng g-1 when treated with the aqueous citric acid. Two major products, produced … …American Journal of Agricultural and Biological Sciences, Vol. 3, Issue 2 · 30 Jun 2008 · 8,049 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleDetermination of Pesticide Residues in Banana by Using High Performance Liquid Chromatography and Gas Chromatography-Mass SpectrometryR. Paranthaman, A. Sudha, S. KumaravelProblem statement: The occurrence of endosulfan, carbendazim, chloropyripos in 10 banana samples in southern area of Tamilnadu, India (hill banana, karpuravalli, monthan, nendran, ney poovan, pachanadan, poovan, rasthali, red banana, robusta) was investigated. Approach: In 7 samples, Carbendazim was found at concentrations ranging from 0.002-0.11 mg kg-1. In three samples, carbendazim was not found, whereas endosulfan, chloropyripos was not detected … …American Journal of Biochemistry and Biotechnology, Vol. 8, Issue 1 · 1 Mar 2012 · 9,544 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleIdentification of Perfluorooctanoic Acid Release from Commercial Coated Cooking Pans by Liquid Chromatography Coupled to Electrospray Ionization Tandem Mass SpectrometryMonica Bononi, Fernando TateoSalts of perfluorooctanoic acid (PFOA) can be used in the manufacture of fluoropolymers employed for coating pans; moreover, PFOA can be formed as a byproduct of thermolysis of the aforesaid fluoropolymers. This study was carried out to evaluate PFOA migration into food cooked in fluoropolymer-coated pans. The pans were purchased from a local retailer and subjected to cooking conditions. Used … …American Journal of Agricultural and Biological Sciences, Vol. 2, Issue 3 · 30 Sep 2007 · 8,221 accessesView PDFCite
Research ArticleOpen accessPhrase in the title2-Nonenal-Ovulatory Specific Volatiles in Human Saliva throughout Menstrual Cycle by Gas Chromatography and Mass Spectrometry AnalysisS. Alagendran, G. Archunan, K. Rameshkumar et al.Problem statement: The present investigation carry out a pilot study of a novel method to identify the salivary volatiles in different phases of menstrual cycle for the assessment of ovulation detection using gas chromatography and mass spectrophotometer. Approach: The profiles from follicular phase (6-12 days); ovulatory phase (13-14 days) and luteal phase (15-26 days) of menstrual cycle samples were compared … …American Journal of Biochemistry and Biotechnology, Vol. 6, Issue 3 · 30 Sep 2010 · 8,365 accessesView PDFCite
Research ArticleOpen accessIn the keywordsIntegrated Monitoring of Endocrine-Disrupting Chemicals: Analytical Chemistry and Biological Assessment ApproachesChangjin Li, Jing Huo, Zijun Dou et al.Endocrine-Disrupting Chemicals (EDCs) in aquatic environments pose significant threats to ecosystems and human health. These compounds interfere with hormonal regulation at low concentrations and have non-monotonic dose-response relationships, posing challenges to conventional risk assessment. This review systematically compares current EDC monitoring methods, including instrumental chemical analysis and receptor-based biological detection systems, to evaluate sensitivity thresholds, sample throughput, and mechanistic selectivity … …American Journal of Biochemistry and Biotechnology, Vol. 22, Issue 2 · 3 Jul 2026 · 1,081 accessesView PDFCite
Research ArticleOpen accessIn the keywordsExtraction, Partial Identification and Bioactivities of Total Flavonoids from Carex meyeriana KunthHongbiao Wang, Penghui Wang, Xiudong Yang et al.To date, knowledge associated with extraction, chemical constituents and bioactivities of Total Flavonoids from Carex meyeriana Kunth (TFCMK) that remains unclear. Therefore, this paper was designed to optimize the ethanol reflux extraction method by response surface methodology and determine the chemical constituents by Liquid Phase-Mass Spectrometry (HPLC-MS); additionally, the bioactivities including antioxidant, antibacterial and hemolysis test were also explored. The … …American Journal of Biochemistry and Biotechnology, Vol. 15, Issue 3 · 7 Aug 2019 · 7,523 accessesView PDFCite
Research ArticleOpen accessIn the keywordsRETRACTED: Analysis of Interfering Substances in the Measurement of Malondialdehyde Content in Plant LeavesYunSheng Wang, MaoDi Ding, XunGang Gu et al.The Thiobarbituric Acid (TBA) reactive substances assay is an easy and quick assay for the assessment in plants of lipid peroxidation, in which Malondialdehyde (MDA) is derivatized. To analyze the applicability of this method, the MDA concentrations in the leaves of different plants were measured by the TBA method. To further separate the interfering substances, fractional extraction and Gas Chromatography-Mass … …American Journal of Biochemistry and Biotechnology, Vol. 9, Issue 3 · 21 Sep 2013 · 9,288 accessesView PDFCite
Research ArticleOpen accessIn the keywordsPhysico-Chemical Characteristics of Date Seed Oil Grown in SudanRehab Salih Mahmoud Abdalla, Alsheikh AlGilani Albasheer, Abdel Rahim Mohamed ELHussein, ELrasheed Ahmed GadkariemProblem statement: Studies were conducted on the physical-chemical properties of Sudanese date seed oil extracted from two date palm cultivars (Phoenix dactylifera L.) ALBarakawi and Alqundeila. The extracted oil from ALBarakawi seeds weighed 6.833% w/w oil, Alqundeila oil extracted weighed 5.064% w/w. Approach: The physical properties of ALBarakawi oil were: viscosity: 17cp, refractive Index: 1.444, density: 0.9116 g cm-3 color: … …American Journal of Applied Sciences, Vol. 9, Issue 7 · 5 May 2012 · 9,500 accessesView PDFCite
Research ArticleOpen accessIn the keywordsCharacterization of Epoxidized and Non-Epoxidized Fatty Diethanolamides by High Performance Liquid Chromatography and Gas ChromatographyChoy Sin Lee, Song Cang LeeProblem statement: This study was carried out for the characterization of epoxidized and non-epoxidized fatty diethanolamides by High Performance Liquid Chromatography (HPLC) and Gas Chromatography (GC). Approach: The fatty diethanolamides were synthesized by reacting 40% (w/w) of Epoxidized Palm Olein (EPOo) with 60% (w/w) Refined Bleached Deodorized Plam Kernel Olein (RBDPKOo) with Diethanolamine (DEA) at 110°C for 5 h. Results: … …American Journal of Pharmacology and Toxicology, Vol. 5, Issue 3 · 30 Sep 2010 · 7,449 accessesView PDFCite
Research ArticleOpen accessIn the keywordsMetabolic Fingerprinting of Three Malaysian Ginger (Zingiber officinale Roscoe) Using Gas Chromatography-Mass SpectromertryH.J. Mahdi, R. Andayani, IshakProblem statement: There is a chemical variation among different ginger cultivars detected by previous studies including the volatile and non-volatile oleo-resins. In this study we try to determine whether these variations are related to a genetic factor rather than environmental or intrinsic factors. Approach: A comprehensive metabolic fingerprinting from the leaves of three micro-propagated ginger cultivars Bukit Tinggi, Tanjung Sepat … …American Journal of Applied Sciences, Vol. 7, Issue 1 · 31 Jan 2010 · 7,387 accessesView PDFCite