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169 articles for “chromatograph”
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Research ArticleOpen accessEvery word in the titleCharacteristics of Lipoprotein Peak x Eluted from a Column with the Eluent of High-magnesium Ion Concentration in Lipoprotein Analysis Using the Cation-exchange ChromatographyYuji Hirowatari, Hiroshi Yoshida, Yutaka Ogura et al.The new lipoprotein analysis method using a cation-exchange chromatography, which contains a sulfopropyl-ligand column and two magnesium ion-containing eluents was previously reported. This method can separate serum lipoproteins on the column gel with a magnesium ion concentration gradient and high-density lipoprotein (HDL), low-density lipoprotein (LDL), very-low-density lipoprotein (VLDL) and an unspecified lipoprotein peak are eluted in order from the column. … …American Journal of Biochemistry and Biotechnology, Vol. 1, Issue 3 · 30 Sep 2005 · 6,477 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Pesticide Residues in Banana by Using High Performance Liquid Chromatography and Gas Chromatography-Mass SpectrometryR. Paranthaman, A. Sudha, S. KumaravelProblem statement: The occurrence of endosulfan, carbendazim, chloropyripos in 10 banana samples in southern area of Tamilnadu, India (hill banana, karpuravalli, monthan, nendran, ney poovan, pachanadan, poovan, rasthali, red banana, robusta) was investigated. Approach: In 7 samples, Carbendazim was found at concentrations ranging from 0.002-0.11 mg kg-1. In three samples, carbendazim was not found, whereas endosulfan, chloropyripos was not detected … …American Journal of Biochemistry and Biotechnology, Vol. 8, Issue 1 · 1 Mar 2012 · 9,548 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDirect Analysis of Six Pharmaceuticals using Online Solid Phase Extraction Liquid ChromatographySiti Norbayu Mohd Subari, Rozita Osman, Norashikin SaimIn this study, three parameters (sample volume, cleanup and elution step) in large volume injection online Solid Phase Extraction Liquid Chromatography with diode array detection (SPE-LC) were optimized for the determination of six pharmaceuticals in wastewater samples. Preconcentration and separation were carried out using 2 columns, Dionex Ion Pac AG14A and Acclaim Polar Advantage II. Response Surface Methodology (RSM) was … …American Journal of Applied Sciences, Vol. 14, Issue 5 · 31 Mar 2017 · 7,518 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleThe Comparison of Spectrophotometric Method and High-Performance Liquid Chromatography in Photosynthetic Pigments AnalysisSabina Jodłowska, Adam LatałaProblem statement: Spectrophotometric method and High-Performance Liquid Chromatography (HPLC) are the most useful tools to photosynthetic pigments analysis. The main objective of this reaserch was to compere the results obtained by these two independent methods in experiments under controlled laboratory conditions. Approach: Comparison between spectrophotometric and HPLC methods for pigment analysis was carried out on Baltic cyanobacterium Geitlerinema amphibium, which … …OnLine Journal of Biological Sciences, Vol. 11, Issue 2 · 30 Sep 2011 · 10,872 accessesView PDFCite
Research ArticleOpen accessEvery word in the title2-Nonenal-Ovulatory Specific Volatiles in Human Saliva throughout Menstrual Cycle by Gas Chromatography and Mass Spectrometry AnalysisS. Alagendran, G. Archunan, K. Rameshkumar et al.Problem statement: The present investigation carry out a pilot study of a novel method to identify the salivary volatiles in different phases of menstrual cycle for the assessment of ovulation detection using gas chromatography and mass spectrophotometer. Approach: The profiles from follicular phase (6-12 days); ovulatory phase (13-14 days) and luteal phase (15-26 days) of menstrual cycle samples were compared … …American Journal of Biochemistry and Biotechnology, Vol. 6, Issue 3 · 30 Sep 2010 · 8,369 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleChemical Profile of Sotol Analyzed by Solid Phase Microextraction-Gas ChromatographyHeliodoro de la Garza, Juan Buenrostro, María Reyes-Vega et al.Problem statement: Sotol is a distilled spirit made from Dasylirion spp., a plant (called sotol) that grows in the wilds of Northern Mexico and west Texas and New Mexico. This alcoholic beverage is produced in a similar process to the more common artisanal tequila and mescal. Sotol is also now beginning to achieve international recognition; however there are few commercial … …American Journal of Agricultural and Biological Sciences, Vol. 5, Issue 3 · 30 Sep 2010 · 8,340 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleIdentification of Perfluorooctanoic Acid Release from Commercial Coated Cooking Pans by Liquid Chromatography Coupled to Electrospray Ionization Tandem Mass SpectrometryMonica Bononi, Fernando TateoSalts of perfluorooctanoic acid (PFOA) can be used in the manufacture of fluoropolymers employed for coating pans; moreover, PFOA can be formed as a byproduct of thermolysis of the aforesaid fluoropolymers. This study was carried out to evaluate PFOA migration into food cooked in fluoropolymer-coated pans. The pans were purchased from a local retailer and subjected to cooking conditions. Used … …American Journal of Agricultural and Biological Sciences, Vol. 2, Issue 3 · 30 Sep 2007 · 8,224 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleTotal Petroleum Hydrocarbons By Gas Chromatography in Colombian Waters and SoilsC.. González, S. Roa, A. Suspes et al.Total Petroleum Hydrocarbons (TPHs) were required by the Colombian Environmental Authorities. However, the great diversity of hydrocarbon sources, in addition to the variety of available techniques and analytical methods had created confusion among the users of the data in regards to the appropriate methodologies. This study presents the results obtained in the method validation for the determination of TPHs in … …American Journal of Environmental Sciences, Vol. 8, Issue 4 · 20 Jun 2012 · 9,218 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Metoprolol and Felodipine in Binary Mixture Using Chemometric-Assisted Spectrophotometric and High-Performance Liquid Chromatographic-UV MethodsHesham Salem, Ola M. AbdallahFour methods were developed for simultaneous determination of metoprolol and felodipine without previous separation. In the first method both drugs were determined using first derivative UV spectrophotometry, with zero crossing measurement at 222 and 235 nm for metoprolol and felodipine, respectively. The second method depends on first derivative of the ratios spectra by measurements of the amplitudes at 250.1 nm … …American Journal of Applied Sciences, Vol. 4, Issue 9 · 30 Sep 2007 · 8,028 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Diloxanide Furoate and Metronidazole in Binary Mixture Using First Derivative of the Ratio-Spectra and High-Performance Liquid Chromatography-UV MethodsNora H. Al-ShaalanTwo methods are presented for simultaneous determination of diloxanide furoate and metronidazole. The first method depends on first derivative of the ratio-spectra by measurements of the amplitudes at 242.5 and 285.5 nm for diloxanide furoate and 225.5 and 300 nm for metrinidazole. Calibration graphs were established for 2-100 μg mL-1 for diloxanide furoate and 1-50 μg mL-1 for metronidazole. In … …American Journal of Applied Sciences, Vol. 4, Issue 2 · 28 Feb 2007 · 7,719 accessesView PDFCite