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Research ArticleOpen accessIn the keywordsDirect Analysis of Six Pharmaceuticals using Online Solid Phase Extraction Liquid ChromatographySiti Norbayu Mohd Subari, Rozita Osman, Norashikin SaimIn this study, three parameters (sample volume, cleanup and elution step) in large volume injection online Solid Phase Extraction Liquid Chromatography with diode array detection (SPE-LC) were optimized for the determination of six pharmaceuticals in wastewater samples. Preconcentration and separation were carried out using 2 columns, Dionex Ion Pac AG14A and Acclaim Polar Advantage II. Response Surface Methodology (RSM) was … …American Journal of Applied Sciences, Vol. 14, Issue 5 · 31 Mar 2017 · 7,513 accessesView PDFCite