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60 articles for “Liquid chromatography”
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Research ArticleOpen accessPhrase in the titleValidated High Performance Liquid Chromatographic Method for Analysis of Fenvalerate Pesticide in Chilies by QuEChERS Extraction Cleanup and High Liquid ChromatographyAhmed Ambarak Altorshani, Nor Kartini Abu Bakar, Eltayeb Elamin M. EidProblem statement: Contamination associated with pesticide use has increased as well, adversely impacting the environment and causing human health risks through residues on food. Approach: This study reports the extraction of Fenvalerate (FE) in chilies using QuEChERS based on High Performance Liquid Chromatography (HPLC) describes a simple, fast and inexpensive method. The chillie was extracted with acetonitrile Aliquots were cleaned-up … …American Journal of Applied Sciences, Vol. 7, Issue 12 · 31 Dec 2010 · 7,163 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleCharacterization of Epoxidized and Non-Epoxidized Fatty Diethanolamides by High Performance Liquid Chromatography and Gas ChromatographyChoy Sin Lee, Song Cang LeeProblem statement: This study was carried out for the characterization of epoxidized and non-epoxidized fatty diethanolamides by High Performance Liquid Chromatography (HPLC) and Gas Chromatography (GC). Approach: The fatty diethanolamides were synthesized by reacting 40% (w/w) of Epoxidized Palm Olein (EPOo) with 60% (w/w) Refined Bleached Deodorized Plam Kernel Olein (RBDPKOo) with Diethanolamine (DEA) at 110°C for 5 h. Results: … …American Journal of Pharmacology and Toxicology, Vol. 5, Issue 3 · 30 Sep 2010 · 7,449 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleAnalysis of Some Pesticide Residues in Cauliflower by High Performance Liquid ChromatographySheheli Islam, Nazneen Afrin, Mohammad Shawkat Hossain et al.Problem statement: Increased use of chemicals on vegetables started gaining momentum and continued its up-trend in Bangladesh. Wide spread use of pesticides in agriculture concern of residue accumulation, which may remain in food and agricultural environment causing concern of human health and risking ecological balance. Attempt made to ensure that their applications were correct and safe and result in no … …American Journal of Environmental Sciences, Vol. 5, Issue 3 · 30 Jun 2009 · 7,859 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleDirect Analysis of Six Pharmaceuticals using Online Solid Phase Extraction Liquid ChromatographySiti Norbayu Mohd Subari, Rozita Osman, Norashikin SaimIn this study, three parameters (sample volume, cleanup and elution step) in large volume injection online Solid Phase Extraction Liquid Chromatography with diode array detection (SPE-LC) were optimized for the determination of six pharmaceuticals in wastewater samples. Preconcentration and separation were carried out using 2 columns, Dionex Ion Pac AG14A and Acclaim Polar Advantage II. Response Surface Methodology (RSM) was … …American Journal of Applied Sciences, Vol. 14, Issue 5 · 31 Mar 2017 · 7,513 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleThe Comparison of Spectrophotometric Method and High-Performance Liquid Chromatography in Photosynthetic Pigments AnalysisSabina Jodłowska, Adam LatałaProblem statement: Spectrophotometric method and High-Performance Liquid Chromatography (HPLC) are the most useful tools to photosynthetic pigments analysis. The main objective of this reaserch was to compere the results obtained by these two independent methods in experiments under controlled laboratory conditions. Approach: Comparison between spectrophotometric and HPLC methods for pigment analysis was carried out on Baltic cyanobacterium Geitlerinema amphibium, which … …OnLine Journal of Biological Sciences, Vol. 11, Issue 2 · 30 Sep 2011 · 10,865 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleIdentification of Perfluorooctanoic Acid Release from Commercial Coated Cooking Pans by Liquid Chromatography Coupled to Electrospray Ionization Tandem Mass SpectrometryMonica Bononi, Fernando TateoSalts of perfluorooctanoic acid (PFOA) can be used in the manufacture of fluoropolymers employed for coating pans; moreover, PFOA can be formed as a byproduct of thermolysis of the aforesaid fluoropolymers. This study was carried out to evaluate PFOA migration into food cooked in fluoropolymer-coated pans. The pans were purchased from a local retailer and subjected to cooking conditions. Used … …American Journal of Agricultural and Biological Sciences, Vol. 2, Issue 3 · 30 Sep 2007 · 8,221 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleDetermination of Pesticide Residues in Banana by Using High Performance Liquid Chromatography and Gas Chromatography-Mass SpectrometryR. Paranthaman, A. Sudha, S. KumaravelProblem statement: The occurrence of endosulfan, carbendazim, chloropyripos in 10 banana samples in southern area of Tamilnadu, India (hill banana, karpuravalli, monthan, nendran, ney poovan, pachanadan, poovan, rasthali, red banana, robusta) was investigated. Approach: In 7 samples, Carbendazim was found at concentrations ranging from 0.002-0.11 mg kg-1. In three samples, carbendazim was not found, whereas endosulfan, chloropyripos was not detected … …American Journal of Biochemistry and Biotechnology, Vol. 8, Issue 1 · 1 Mar 2012 · 9,544 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleDetermination of Diloxanide Furoate and Metronidazole in Binary Mixture Using First Derivative of the Ratio-Spectra and High-Performance Liquid Chromatography-UV MethodsNora H. Al-ShaalanTwo methods are presented for simultaneous determination of diloxanide furoate and metronidazole. The first method depends on first derivative of the ratio-spectra by measurements of the amplitudes at 242.5 and 285.5 nm for diloxanide furoate and 225.5 and 300 nm for metrinidazole. Calibration graphs were established for 2-100 μg mL-1 for diloxanide furoate and 1-50 μg mL-1 for metronidazole. In … …American Journal of Applied Sciences, Vol. 4, Issue 2 · 28 Feb 2007 · 7,713 accessesView PDFCite
Research ArticleOpen accessIn the keywordsAcer Buergerianumas a New Resource for the Extraction of Corilagin: Determination of Corilaginin Different Cultivars of A. Buergerianumby UPLCQian Qiao, Chong Wu, Jiangyong Wang et al.Corilagin is a promising anticancer drug candidate. Acer nikoense and A. ammonium are both known to contain corilagin. To explore whether corilagin occurs in congeneric species and to fully develop the medicinal value of maple, the corilagin content in different varieties of maple was determined by Ultrahigh-Performance Liquid Chromatography (UPLC). Acer buergerianum leaves contained corilagin and the corilagin content in … …American Journal of Biochemistry and Biotechnology, Vol. 18, Issue 2 · 12 May 2022 · 5,704 accessesView PDFCite
Research ArticleOpen accessIn the keywordsDetermination of Abscisic Acid and its Relationship to Drought Stress Based on Cowpea Varieties with Different Capability of Drought ResistanceWei Lei, Shian Huang, Shaohu Tang et al.Cowpea (Vigna unguiculata L.) is one of the most important grain legume supplying necessarily dietary proteins. Although its can tolerate drought environment, still the severe condition can limit the growth and development of this plant. Abscisic acid (ABA) has a crucial function in stress physiology, but little information is available for methods describing ABA determination in cowpea and its relationship … …American Journal of Biochemistry and Biotechnology, Vol. 12, Issue 1 · 30 Mar 2016 · 8,458 accessesView PDFCite