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90 articles for “Electron Microscopy”

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Research ArticleOpen accessIn the abstractFrom Structural Colors to Super-Hydrophobicity and Achromatic Transparent Protective Coatings: Ion Plating Plasma Assisted TiO2 and SiO2 Nano-Film DepositionRaffaella Aversa, Valeria Perrotta, Relly Victoria V. Petrescu et al.The implementation of the Ion Plating Plasma Assisted technology in the area of surface functionalization for structural color and relic preservation applications is presented. Interferometric structural colors on irregular bumped Titanium surfaces and transparent and achromatic nano films on ancient ceramic artifact have been investigated. Titanium metal and ceramic supports have been utilized for the surface functionalization tests: A metallic … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 4 · 24 Nov 2016 · 8,459 accessesView PDFCite
Research ArticleOpen accessIn the abstractHydrothermal Synthesis of CuWO4-Reduced Graphene Oxide Hybrids and Supercapacitor ApplicationKoyal Suman Samantaray, Surjit Sahoo, Chandra Sekhar RoutThis study reports a facile hydrothermal synthesis of Copper tungsten oxide (CuWO4) and CuWO4-reduced graphene oxide hybrid nanoparticles and its application as an electrode for supercapacitor application. The morphology and composition has been characterized using X-Ray Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM) and EDAX. The supercapacitive behavior has been studied from cyclic voltammetry and galvanostatic charge-discharge tests. The … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 3 · 12 Aug 2016 · 9,554 accessesView PDFCite
Research ArticleOpen accessIn the abstractMixed Nickel Cobalt Manganese Oxide Nanorods for supercapacitor applicationRajat Mondal, Surjit Sahoo, Chandra Sekhar RoutMixed Nickel Cobalt Manganese oxide (NiCoMn-Oxide) is a new class of excellent material for supercapacitor application. Here, hydrothermal synthesis technique has been employed to prepare mixed NiCoMn-Oxide nanorods. The elemental composition and morphology of this material were validated by X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and EDX techniques. To analyze the capacitive performance of this material, cyclic voltammetry and … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 3 · 22 Jun 2016 · 9,044 accessesView PDFCite
Research ArticleOpen accessIn the abstractEffect of Nano-Alumina on Pore Structure and Durability of Class F Fly Ash Self-Compacting MortarEhsan Mohseni, Konstantinos Daniel TsavdaridisIn this study the effect of pore structure on the mechanical properties and durability characteristics of Self-Compacting Mortars (SCM) containing nano-Al2O3 (NA) and class F fly ash are investigated. Al2O3 nanoparticles with the maximum size of 15 nm in three different proportions of 1, 3 and 5% of the binder content were utilized to partially replace the cement. The 25% … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 2 · 14 Apr 2016 · 9,472 accessesView PDFCite
Research ArticleOpen accessIn the abstractEffect of Nano Silica on the Compressive Strength of Harden Cement Paste at Different Stages of HydrationJustin Montgomery, Taher M. Abu-Lebdeh, Sameer A. Hamoush, Miguel PicornellThis study investigated the compressive strength of hardened cement paste and the formation of Calcium Silicate Hydrate (C-S-H) with the addition of nano silica (SiO2). Compressive strength testing was performed using MTS and Forney testing machines to determine stress-strain curves and compressive strength of the materials. The hydration process and formation of C-S-H and Calcium Hydroxide (CH) was examined using … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 1 · 13 Mar 2016 · 8,333 accessesView PDFCite
Research ArticleOpen accessIn the abstractPorosity Analysis in Porous Brass Using Dual ApproachesRyan Yeargin, Rob Ramey, Cindy WatersThe goal of this research is to produce porous samples for various applications such as heat exchangers, filters and radiation shields. The level of porosity is an important objective yet the level of confidence in two main methods (hand calculations and microscopic analysis) is not high. This work will compare porosity values obtained from traditional hand calculations against analysis from … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 1 · 25 Feb 2016 · 8,525 accessesView PDFCite
Research ArticleOpen accessIn the abstractA Clean-Green Synthesis of Platinum Nanoparticles Utilizing a Pernicious Weed Lantana (Lantana Camara)Musthafa O. Mavukkandy, Sudip Chakraborty, Tasneem Abbasi, Shahid A. AbbasiA rapid, reproducible single step method is proposed for synthesizing platinum nanoparticles using an invasive weed lantana (Lantana camara, L). The method involves mixing of platinum (VI) solution, lantana leaf extract and ascorbic acid in appropriate concentrations and keeping the mixture at 95°C for 8 min. The collective action of ascorbic acid and leaf extract reduced the chloroplatinic acid to … …American Journal of Engineering and Applied Sciences, Vol. 9, Issue 1 · 23 Feb 2016 · 10,447 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Marine Clay-Supported Nano Zero Valent IronHo Kuok How, Wan Zuhairi Wan YaacobThis study reports the preparation and characterization of marine clay nano zero valent iron (MC+nZVI) where marine clay acts as the composite material. Marine clay was air dried and pulverized before used. Basically, MC+nZVI was synthesized by chemical reduction method. The materials synthesized were left oven dried overnight at 50°C. The obtained materials were characterized by Field Emission Scanning Electron … …American Journal of Environmental Sciences, Vol. 11, Issue 2 · 26 Jun 2015 · 7,124 accessesView PDFCite
Research ArticleOpen accessIn the abstractRemoval of Copper from Aqueous Solution using Tunisian ClayN. Boujelben, S. Gharab, F. Bouhamed et al.Natural adsorbents such as clay was used to replace expensive imported synthetic adsorbents. In this study, Scanning Electron Microscopy (SEM), Infrared spectroscopy and X-ray diffraction techniques were used to characterize the used sorbent (clays C). Batch experiments were performed to evaluate the effects of contact time, solution pH and temperature on copper removal onto used sorbent from aqueous solution. Equilibrium … …American Journal of Environmental Sciences, Vol. 11, Issue 2 · 15 Jun 2015 · 7,182 accessesView PDFCite
Research ArticleOpen accessIn the abstractFacile Synthesis of AgCl Hollow Nanospheres for Enhanced Photocatalytic PropertiesJing Chen, Yuling Zhao, Xinhui Liu et al.AgCl hollow nanospheres have been synthesized successfully via a hard-template approach using silica nanospheres as hard template for the first time. The phase, size and morphology of the as-prepared AgCl were investigated by X-Ray Diffraction (XRD), Field-Emission Scanning Electron Microscopy (FESEM); which reveals that the cubic AgCl hollow nanospheres with a cell constant a = 5.549 Å are 220 nm … …American Journal of Engineering and Applied Sciences, Vol. 8, Issue 3 · 22 May 2015 · 7,350 accessesView PDFCite