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71 articles for “X-ray analysis”
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Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organotin(IV) N-Benzyl-N-Isopropyldithiocarbamate Compounds: Cytotoxic Assay on Human Hepatocarcinoma Cells (HepG2)Normah Awang, Ibrahim Baba, Nor Syaidatul Akmal Mohd Yousof, Nurul Farahana KamaludinProblem statement: Several studies on organotin(IV) dithiocarbamate compounds have been carried out but not on the synthesis and characterization together with cytotoxic assay of organotin(IV) N-benzyl-N-isopropyldithiocarbamate compounds. Approach: Three new organotin(IV) compounds of type N-benzyl-N-isopropyldithiocarbamate have been successfully synthesized by direct reaction between secondary amine with organotin(IV) chloride using in situ method. All the compounds were characterized using elemental analysis, … …American Journal of Applied Sciences, Vol. 7, Issue 8 · 31 Aug 2010 · 8,092 accessesView PDFCite
Research ArticleOpen accessIn the abstractStandardization of Metal-Based Herbal MedicinesArun Sudha, V. S. Murty, T. S. ChandraProblem statement: Standardization of herbal drugs is a burning topic in herbal drug industry today. Standardization is difficult because they are usually mixtures of many constituents and the active principle in most cases is unknown. However it is possible to generate a physico-chemical fingerprint for the standardization of these drugs with reference to authentic drugs, for monitoring variation between preparations … …American Journal of Infectious Diseases, Vol. 5, Issue 3 · 30 Sep 2009 · 7,904 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis of Al3Fe5O12 Cubic Structure by Extremely Low Sintering Temperature of Sol Gel TechniqueNoorhana Yahya, Ramadan A.H. Masoud, Hanita Daud et al.Problem statement: Fabrication of nano materials particularly nano inductors at low sintering temperature remains a challenge. This study was carried out as our initial response to obtain a nano-size inductors, which is aluminium iron garnet using low sintering temperature. Approach: The aluminum iron garnet (Al3Fe5O12) nano crystals were prepared by sol-gel technique. The starting solution is a mixture of iron … …American Journal of Engineering and Applied Sciences, Vol. 2, Issue 1 · 31 Mar 2009 · 8,563 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis of Mesoporous Titania with Surfactant and its CharacterizationT. Benkacem, N. AgoudjilA mesoporous titania was obtained by gelation from Ti-alkoxide in acidic solutions with addition of surfactant cetyltrimetylammonium bromide (CH3(CH2)15N(CH3)3Br) using a sol-gel process. The effects of surfactant concentration on synthesis of mesoporous titania were studied. The structural characterisation was studied by differential thermal analysis, infrared spectroscopy, X-ray diffraction. Studies by X-ray diffraction showed that crystallisation of TiO2 powder occurs at … …American Journal of Applied Sciences, Vol. 5, Issue 11 · 30 Nov 2008 · 7,414 accessesView PDFCite
Research ArticleOpen accessIn the abstractNovel Metal Accumulator and Protease Secretor Microbes from East Calcutta WetlandSanhita Chowdhury, Madhusmita Mishra, V.K. Adarsh et al.Nine bacterial isolates were screened from different sites of East Calcutta Wetland, an ecosystem located at the eastern fringes of Calcutta. Other than being a biodiversity rich area, the important feature of this system is that it is a natural sewage treatment plant for the city of Calcutta. In addition to daily sewage including solid and soluble wastes, a considerable … …American Journal of Biochemistry and Biotechnology, Vol. 4, Issue 3 · 30 Sep 2008 · 8,987 accessesView PDFCite
Research ArticleOpen accessIn the abstractEffect of Film thickness on the Electrical and Structural Properties of CdS: In Thin FilmsShadia J. Ikhmayies, Riyad N. Ahmad-BitarPolycrystalline CdS:In thin films were prepared by the Spray Pyrolysis (SP) technique on glass substrates at a substrate temperature Ts= 490°C. The effect of film thickness on the electrical and structural properties of the films was investigated through the analysis of the I-V plots, x-ray diffraction spectra (XRD) and the scanning electron microscope (SEM) images. The conductivity of the films … …American Journal of Applied Sciences, Vol. 5, Issue 9 · 30 Sep 2008 · 6,910 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Charaterization of Magnesium Zinc Ferrites as Electromagnetic SourceNoorhana Yahya, Ami Salwani Mohamad Nor Aripin, Azizuddin A. Aziz et al.Fabrication of Mg1-XZnXFe2O4 (where x = 0.2, 0.3, 0.4 and 0.5) samples using a conventional technique is reported. Oxides of magnesium, zinc and iron with purity of about 99.99% were mixed with distilled water in a milling machine for 12 hours. They were then filtered and presintered at 1250°C and sintered at 1350°C for 10 h in air. The phase … …American Journal of Engineering and Applied Sciences, Vol. 1, Issue 1 · 31 Mar 2008 · 8,998 accessesView PDFCite
Research ArticleOpen accessIn the abstractStudies on Metal Microbe Interaction of Three Bacterial Isolates From East Calcutta WetlandV. K. Adarsh, Madhusmita Mishra, Sanhita Chowdhury et al.The present paper put forth the isolation and complete characterization of three bacterial isolates from different sites of East Calcutta Wetland (ECW). These isolates show tolerance to heavy metals like Ag, Al, Cu, Cr, Co, Ni, Pb and were found to be efficient metal accumulators as evident from Energy Dispersive X Ray Fluorescence (EDXRF) analysis and Transmission Electron Microscopy (TEM). … …OnLine Journal of Biological Sciences, Vol. 7, Issue 2 · 31 Dec 2007 · 9,423 accessesView PDFCite
Research ArticleOpen accessIn the abstractTracking Error Analysis of a Rotation-Elevation Mode HeliostatOmar Aliman, Ismail Daut, Muzamir Isa, Mohd Rafi AdzmanFor the past few years, great efforts have been done in improving the tracking accuracy of a newly proposed rotation-elevation tracking mode heliostat. A special simulation program has been developed to systematically analyze the image movement and to find out the error of the parameters. In the simulation program, ray-tracing method was applied to work out the central point position … …American Journal of Applied Sciences, Vol. 4, Issue 3 · 31 Mar 2007 · 7,251 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organoclay from Sodium Montmorillonite and Fatty Hydroxamic AcidsWisam H. Hoidy, Mansor B. Ahmad, Emad A. Jaffar Al Mulla, Nor Azowa Bt IbrahimProblem statement: Sodium Montmorillonite (Na-MMT) has been modified via cation exchange reaction using Fatty Hydroxamic Acids (FHAs) synthesized from palm oil as a surfactant to produce organoclay which is used to prepare polymer nanocomposites. Approach: Basal spacing, functional groups identification and thermal stability of this Organo-Montmorillonite (OMMT) were characterized using X-ray Diffraction (XRD), Fourier Transform Infrared (FTIR) spectroscopy and Thermogravimetric … …American Journal of Applied Sciences, Vol. 6, Issue 8 · 31 Aug 2009 · 9,305 accessesView PDFCite