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46 results for “Infrared (IR) Spectroscopy”
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Research ArticleOpen accessIn the abstractSynthesis of Baso4 Nanoparticles by Precipitation Method Using Polycarboxylate as a ModifierMohamed El-Shahate Ismaiel Saraya, Inas Mostafa BakrProblem statement: Barium Sulfate (BaSO4) is suitable for many applications because of its whiteness, inertness and high specific gravity. Approach: Nanoparticles of barium sulphate (BaSO4) have been synthesized from barium nitrate by precipitation method in the presence of water soluble organic polycarboxylic polymer as a modifying agent. Transmission electron microscopy, Scanning electron microscopy, Fourier transform infrared spectroscopy and X-ray powder … …Current Research in Nanotechnology, Vol. 2, Issue 1 · 29 Jul 2011 · 15,705 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis, Characterization and Biological Activities of Organotin (IV) Methylcyclohexyldithiocarbamate CompoundsNormah Awang, Ibrahim Baba, Bohari M. Yamin et al.Problem statement: The growing interest in the chemistry of sulphur donor ligands are due to their encouraging anticancer, antibacterial and antifungal activities as well as their widespread industrial application. Dithiocarbamates belong to this class and much attention has been paid to them. Approach: Novel organotin compounds with the molecular formula RmSn[S2CN(CH3)(C6H11)]4-m (where m = 2, R = CH3, C2H5; m … …American Journal of Applied Sciences, Vol. 8, Issue 4 · 18 Apr 2011 · 9,210 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Calcium Channel Blocking Activity of 1, 4-Dihydropyridine Derivatives Containing Ester Substitute and Phenyl Carbamoyl GroupBassem Sadek, Khairi Mustafa Salem Fahelelbom, Laurentiu Morusciag, Sigurd ElzProblem statement: Several studies on the synthesis of new nifedipine analogs have been carried out, but the literature reveled that no study on the synthesis and calcium channel blocking activity of the substituted ester with an amide (5-phenylcarbamoyl) moiety has been reported. Approach: Six new derivatives of m-nifedipine have been successfully synthesized by substituting an ester moiety with an amide … …American Journal of Applied Sciences, Vol. 8, Issue 4 · 18 Apr 2011 · 8,247 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organotin(IV) N-Benzyl-N-Isopropyldithiocarbamate Compounds: Cytotoxic Assay on Human Hepatocarcinoma Cells (HepG2)Normah Awang, Ibrahim Baba, Nor Syaidatul Akmal Mohd Yousof, Nurul Farahana KamaludinProblem statement: Several studies on organotin(IV) dithiocarbamate compounds have been carried out but not on the synthesis and characterization together with cytotoxic assay of organotin(IV) N-benzyl-N-isopropyldithiocarbamate compounds. Approach: Three new organotin(IV) compounds of type N-benzyl-N-isopropyldithiocarbamate have been successfully synthesized by direct reaction between secondary amine with organotin(IV) chloride using in situ method. All the compounds were characterized using elemental analysis, … …American Journal of Applied Sciences, Vol. 7, Issue 8 · 31 Aug 2010 · 8,092 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organotin(IV) Complexes Derived of 2-amino-5-nitrobenzoic Acid: In vitro Antibacterial Screening ActivityYip-Foo Win, Siang-Guan Teoh, M. R. Vikneswaran et al.Problem statement: Tremendous studies have been carried out on organotin(IV) complexes derivatives of carboxylate anions. However, the synthesis and characterization as well as the in vitro antibacterial screening activity of organotin(IV) carboxylate derived of 2-amino-5-nitrobenzoic acid have not been carried out. Approach: Organotin(IV) carboxylate complexes derivative of 2-amino-5-nitrobenzoic acid, 2-NH2-5-NO2-C6H3COOH have been successfully synthesized. The acid and complexes obtained were … …American Journal of Applied Sciences, Vol. 7, Issue 7 · 31 Jul 2010 · 8,797 accessesView PDFCite
Research ArticleOpen accessIn the abstractSupercritical Ethanol Liquefaction of Swine Manure for Bio-Oils ProductionShuangning Xiu, Abolghasem Shahbazi, Lijun Wang, Carlington W. WallaceProblem statement: Environmental problems associated with animal waste are the most critical challenges faced by the US intensive confinement livestock industries. There is an import and urgent need to develop an efficient way to reduce the pollution of animal waste while extracting valuable energy. Supercritical liquefaction processing of swine manure into a liquid fuel was considered as a cost-effective approach … …American Journal of Engineering and Applied Sciences, Vol. 3, Issue 2 · 30 Jun 2010 · 8,245 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organotin(IV) Complexes Derived of 3-(Dimethylamino)benzoic Acid: Cytotoxic Assay on Human Liver Carcinoma Cells (HepG2)Yip-Foo Win, Siang-Guan Teoh, Tengku-Sifzizul Tengku-Muhammad et al.Problem statement: Many studies have been carried out on organotin(IV) complexes derivative of carboxylate anions. However, the synthesis and characterization as well as the cytotoxic assay of organotin(IV) carboxylate derived of 3-(dimethylamino)benzoic acid have not been studied. Approach: Organotin(IV) carboxylate complexes derivative of 3-(dimethylamino)benzoic acid, 3-[N(CH3)2]C6H4COOH have been successfully synthesized. Two types of diorganotin(IV) complexes, [{3-[N(CH3)2]C6H4COO(R)2Sn}2O]2 dimer (R = methyl … …American Journal of Applied Sciences, Vol. 7, Issue 3 · 31 Mar 2010 · 8,310 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Silver/Clay/Chitosan Bionanocomposites by UV-Irradiation MethodMansor Bin Ahmad, Kamyar Shameli, Majid Darroudi et al.Problem statement: Silver/Montmorillonite/Chitosan Bionanocomposites (Ag/MMT/Cts BNCs) have been synthesized by UV-irradiation reduction method in the absence of any reducing agent or heat treatment which is used to antibacterial application and medical devices. Approach: MMT, Chitosan and AgNO3 were used as a solid support, stabilizer and silver precursor, respectively. The properties of Ag/MMT/Cts BNCs were studied as a function of UV-irradiation … …American Journal of Applied Sciences, Vol. 6, Issue 12 · 31 Dec 2009 · 8,815 accessesView PDFCite
Research ArticleOpen accessIn the abstractStandardization of Metal-Based Herbal MedicinesArun Sudha, V. S. Murty, T. S. ChandraProblem statement: Standardization of herbal drugs is a burning topic in herbal drug industry today. Standardization is difficult because they are usually mixtures of many constituents and the active principle in most cases is unknown. However it is possible to generate a physico-chemical fingerprint for the standardization of these drugs with reference to authentic drugs, for monitoring variation between preparations … …American Journal of Infectious Diseases, Vol. 5, Issue 3 · 30 Sep 2009 · 7,904 accessesView PDFCite
Research ArticleOpen accessIn the abstractSynthesis and Characterization of Organoclay from Sodium Montmorillonite and Fatty Hydroxamic AcidsWisam H. Hoidy, Mansor B. Ahmad, Emad A. Jaffar Al Mulla, Nor Azowa Bt IbrahimProblem statement: Sodium Montmorillonite (Na-MMT) has been modified via cation exchange reaction using Fatty Hydroxamic Acids (FHAs) synthesized from palm oil as a surfactant to produce organoclay which is used to prepare polymer nanocomposites. Approach: Basal spacing, functional groups identification and thermal stability of this Organo-Montmorillonite (OMMT) were characterized using X-ray Diffraction (XRD), Fourier Transform Infrared (FTIR) spectroscopy and Thermogravimetric … …American Journal of Applied Sciences, Vol. 6, Issue 8 · 31 Aug 2009 · 9,305 accessesView PDFCite