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35 results for “HPLC method”
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Research ArticleOpen accessIn the abstractPhysico-Chemical Characteristics of Date Seed Oil Grown in SudanRehab Salih Mahmoud Abdalla, Alsheikh AlGilani Albasheer, Abdel Rahim Mohamed ELHussein, ELrasheed Ahmed GadkariemProblem statement: Studies were conducted on the physical-chemical properties of Sudanese date seed oil extracted from two date palm cultivars (Phoenix dactylifera L.) ALBarakawi and Alqundeila. The extracted oil from ALBarakawi seeds weighed 6.833% w/w oil, Alqundeila oil extracted weighed 5.064% w/w. Approach: The physical properties of ALBarakawi oil were: viscosity: 17cp, refractive Index: 1.444, density: 0.9116 g cm-3 color: … …American Journal of Applied Sciences, Vol. 9, Issue 7 · 5 May 2012 · 9,500 accessesView PDFCite
Research ArticleOpen accessIn the abstractQuantification of Zolpidem in Canine PlasmaMario Giorgi, Alessandra Gavazza, Hyoin YunProblem statement: Zolpidem is a non-benzodiazepine hypnotic agent currently used in human medicine. In contrast to benzodiazepines, zolpidem preferentially binds with the GABAA complex ϖ1 receptors while poorly interacting with the other ϖ receptor complexes. Recent studies have suggested that ZP may be used to initiate sedation and diminish severe anxiety responses in dogs. The aim of the present study … …American Journal of Animal and Veterinary Sciences, Vol. 7, Issue 1 · 19 Mar 2012 · 7,908 accessesView PDFCite
Research ArticleOpen accessIn the abstractThe Comparison of Spectrophotometric Method and High-Performance Liquid Chromatography in Photosynthetic Pigments AnalysisSabina Jodłowska, Adam LatałaProblem statement: Spectrophotometric method and High-Performance Liquid Chromatography (HPLC) are the most useful tools to photosynthetic pigments analysis. The main objective of this reaserch was to compere the results obtained by these two independent methods in experiments under controlled laboratory conditions. Approach: Comparison between spectrophotometric and HPLC methods for pigment analysis was carried out on Baltic cyanobacterium Geitlerinema amphibium, which … …OnLine Journal of Biological Sciences, Vol. 11, Issue 2 · 30 Sep 2011 · 10,865 accessesView PDFCite
Research ArticleOpen accessIn the abstractRelation between Macroscopic Binding Constant and the Anticancer Efficacy of the Bovine Serum Albumin-Quercetin Complex against Drug-Sensitive and Drug-Resistant CellsWinit Choiprasert, Chatchanok Loetchutinat, Nathupakorn Dechsupa, Samlee MankhetkornProblem statement: We have previously analyzed the interaction of BSA with flavonoids by using FRET. In this study, the role of BSA on increasing in solubility and on carrying the quercetin derivatives thus enhanced their anticancer efficacy against drug-sensitive and drug-resistant cells were conducted. Approach: The macroscopic (KD) and microscopic (kd) binding constant of the complexation and the cellular partition … …American Journal of Biochemistry and Biotechnology, Vol. 7, Issue 1 · 27 May 2011 · 8,292 accessesView PDFCite
Research ArticleOpen accessIn the abstractValidated High Performance Liquid Chromatographic Method for Analysis of Fenvalerate Pesticide in Chilies by QuEChERS Extraction Cleanup and High Liquid ChromatographyAhmed Ambarak Altorshani, Nor Kartini Abu Bakar, Eltayeb Elamin M. EidProblem statement: Contamination associated with pesticide use has increased as well, adversely impacting the environment and causing human health risks through residues on food. Approach: This study reports the extraction of Fenvalerate (FE) in chilies using QuEChERS based on High Performance Liquid Chromatography (HPLC) describes a simple, fast and inexpensive method. The chillie was extracted with acetonitrile Aliquots were cleaned-up … …American Journal of Applied Sciences, Vol. 7, Issue 12 · 31 Dec 2010 · 7,163 accessesView PDFCite
Research ArticleOpen accessIn the abstractAnalysis of Some Pesticide Residues in Cauliflower by High Performance Liquid ChromatographySheheli Islam, Nazneen Afrin, Mohammad Shawkat Hossain et al.Problem statement: Increased use of chemicals on vegetables started gaining momentum and continued its up-trend in Bangladesh. Wide spread use of pesticides in agriculture concern of residue accumulation, which may remain in food and agricultural environment causing concern of human health and risking ecological balance. Attempt made to ensure that their applications were correct and safe and result in no … …American Journal of Environmental Sciences, Vol. 5, Issue 3 · 30 Jun 2009 · 7,859 accessesView PDFCite
Research ArticleOpen accessIn the abstractMass Spectrometry/Mass Spectrometry Study on the Degradation of B-Aflatoxins in Maize with Aqueous Citric AcidA. Méndez-Albores, I. Nicolás-Vázquez, R. Miranda-Ruvalcaba, E. Moreno-MartÍnezDegradation of B-aflatoxins in maize by means of 1N aqueous citric acid was confirmed by the AFLATEST immunoaffinity column method, High Performance Liquid Chromatography (HPLC), tandem mass spectrometry (MS/MS) and computational information. The AFLATEST and HPLC assays showed that 96.7% degradation occurred in maize contaminated with 93 ng g-1 when treated with the aqueous citric acid. Two major products, produced … …American Journal of Agricultural and Biological Sciences, Vol. 3, Issue 2 · 30 Jun 2008 · 8,049 accessesView PDFCite
Research ArticleOpen accessIn the abstractDetermination of Metoprolol and Felodipine in Binary Mixture Using Chemometric-Assisted Spectrophotometric and High-Performance Liquid Chromatographic-UV MethodsHesham Salem, Ola M. AbdallahFour methods were developed for simultaneous determination of metoprolol and felodipine without previous separation. In the first method both drugs were determined using first derivative UV spectrophotometry, with zero crossing measurement at 222 and 235 nm for metoprolol and felodipine, respectively. The second method depends on first derivative of the ratios spectra by measurements of the amplitudes at 250.1 nm … …American Journal of Applied Sciences, Vol. 4, Issue 9 · 30 Sep 2007 · 8,025 accessesView PDFCite
Research ArticleOpen accessIn the abstractThe Effect of Physical Refining on Palm Vitamin E (Tocopherol, Tocotrienol and Tocomonoenol)Chiew Wei Puah, Yuen May Choo, Ah Ngan Ma, Cheng Hock ChuahThis study reports the effect of physical refining on palm vitamin E including α- tocopherol, α-, γ and α-tocotrienols as well as α- tocomonoenol. A method using HPLC with fluorescence detector using normal phase silica column is described. An isocratic elution with n-hexane/THF/2-propanol (1000:60:4, by vol.) as mobile phase was used. The structure of the α- tocomonoenol was determined using … …American Journal of Applied Sciences, Vol. 4, Issue 6 · 30 Jun 2007 · 8,362 accessesView PDFCite
Research ArticleOpen accessIn the abstractDetermination of Diloxanide Furoate and Metronidazole in Binary Mixture Using First Derivative of the Ratio-Spectra and High-Performance Liquid Chromatography-UV MethodsNora H. Al-ShaalanTwo methods are presented for simultaneous determination of diloxanide furoate and metronidazole. The first method depends on first derivative of the ratio-spectra by measurements of the amplitudes at 242.5 and 285.5 nm for diloxanide furoate and 225.5 and 300 nm for metrinidazole. Calibration graphs were established for 2-100 μg mL-1 for diloxanide furoate and 1-50 μg mL-1 for metronidazole. In … …American Journal of Applied Sciences, Vol. 4, Issue 2 · 28 Feb 2007 · 7,713 accessesView PDFCite