17 articles for “Differential Scanning Calorimetry”

Set a search alert

Research ArticleOpen accessIn the abstractNew Schiff Bases with Pyridine Core: Spectral, Thermal and Optical CharacterizationsSie-Tiong Ha, Lay-Khoon Ong, Yip-Foo Win et al.Problem statement: Numerous studies have been conducted on the Schiff base's alkyl and alkyloxy possessing aromatic core. However, the thermo tropic properties of Schiff base's ester (or alkanoyloxy) with pyridine core was rare studied. Approach: To study spectral, thermal and optical behaviors of Schiff base ester possessing heterocyclic (pyridine) terminal core. A series of 4-[(pyridin-3-ylmethylene) amino] phenylalkanoates were prepared and … …American Journal of Applied Sciences, Vol. 7, Issue 5 · 31 May 2010 · 7,464 accessesView PDF Cite

Research ArticleOpen accessIn the abstractCharacterization of Nigella Sativa L. Essential Oil-Loaded Solid Lipid NanoparticlesNagi A. ALHaj, Mariana N. Shamsudin, Norfarrah M. Alipiah et al.Problem statement: Seeds of Nigella Sativa L., commonly known as black seed, have been used in traditional medicine by many Asian, Middle Eastern and Far Eastern Countries to treat headache, coughs, abdominal pain, diarrhea, asthma, rheumatism and other diseases. The seeds of this plant are the most extensively studied, both phytochemically and pharmacologically. The aqueous and oil extracts of the … …American Journal of Pharmacology and Toxicology, Vol. 5, Issue 1 · 31 Mar 2010 · 17,874 accessesView PDF Cite

Research ArticleOpen accessIn the abstractNew Mesogenic Schiff Base Esters with Polar Chloro Substituent: Synthesis, Thermotropic Properties and X-Ray Diffraction StudiesSie-Tiong Ha, Lay-Khoon Ong, Yasodha Sivasothy et al.Problem statement: Many studies have been conducted on the Schiff base’s alkyl and alkyloxy possessing terminal halogen substituent. However, the thermotropic properties of Schiff base’s ester (or alkanoyloxy) with chloro terminal group remained unstudied. Approach: Synthesis a series of new Schiff base ester possessing polar chloro group and investigate its mesomorphic properties. The title compounds were prepared via condensation and … …American Journal of Applied Sciences, Vol. 7, Issue 2 · 28 Feb 2010 · 12,956 accessesView PDF Cite

Research ArticleOpen accessIn the abstractHeating Effects on Structural and Electrical Properties of PolyetherimideNissaf Mzabi, Hichem Smaoui, Hajer Guermazi et al.Problem statement: Polyetherimide (PEI) has several uses such as electrical insulation. It can undergo different constraints like heat or high voltage which influence its performances as insulator. In this study, the effects of heating on structural and electrical properties of polyetherimide (Ultem 1000) are studied. Approach: PEI samples were heated at different temperatures below the glass transition temperature (175, 190 … …American Journal of Engineering and Applied Sciences, Vol. 2, Issue 1 · 31 Mar 2009 · 8,550 accessesView PDF Cite

Research ArticleOpen accessIn the abstractEffect of Manufacturing Stresses to Die Attach Film Performance In Quad Flatpack No-Lead Stacked Die PackagesM. F. Rosle, I. Abdullah, S. Abdullah et al.Problem statement: Repeated heat cure during assembly processes affected the Die Attach Film (DAF) material properties and the effectiveness touched area that leads to weak die bonding and delamination. Suitable die attached condition and DAF material selection had been evaluated to achieve required reliability performance in the manufacturing of the 3D Quad Flat No-Lead (QFN) stacked die package. Approach: During … …American Journal of Engineering and Applied Sciences, Vol. 2, Issue 1 · 31 Mar 2009 · 8,048 accessesView PDF Cite

Research ArticleOpen accessIn the abstractPreparation and Properties of Copolyanhydrides Based on 2-Hexadecylsuccinic Acid and Sebacic AcidYousef Hamdan, Xiangmei Jiang, Kaixun Huang, Kaichao YuPoly(2-hexadecylsuccinic acid-sebacic acid) (P(HSA-SA)) copolymers have been prepared by melt polycondensation. The copolymers were characterized by FT-IR, 1HNMR, gel permeation chromatography (GPC), differential scanning calorimetry (DSC) and thermal gravimetric analysis (TGA). In vitro studies showed that all our prepared copolymers are degradable in phosphate buffer at 37°C. The release profiles of hydrophilic model drug, ciprofloxcin hydrochloride, from the copolymers, follow … …American Journal of Applied Sciences, Vol. 4, Issue 3 · 31 Mar 2007 · 7,427 accessesView PDF Cite

Research ArticleOpen accessIn the abstractIdentification, Characterization and Quantification of Elastomeric/Plastomeric Waste for Sustainable Waste MinimizationKajal Yadav, Sangita, A. ChandraThe present study focuses on the importance of characterization of waste/post consumer polymers. In recent years sophisticated instrumental techniques played an important role in identification and characterization of polymers. Advances in computer techniques have been combined with analytical instruments to give analytical speed, resolution and minimal sample requirements unimagined a few years ago. The present study deals with the development … …American Journal of Environmental Sciences, Vol. 1, Issue 3 · 30 Sep 2005 · 7,056 accessesView PDF Cite