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405 articles for “Determination”
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Research ArticleOpen accessEvery word in the titleNovel LC-MS/MS Method for CJ-023423 (Grapiprant) Determination in Rabbit PlasmaElena Baralla, Virginia De Vito, Maria Vittoria Varoni et al.Grapiprant is a new anti-inflammatory drug that preferentially targets the EP4 receptor of prostaglandin E2 limiting the wide range of adverse effects caused by the classical non steroideal anti-inflammatory drugs. The aim of this study was to develop and validate a new, simple, sensitive and rapid Liquid Chromatography tandem Mass Spectrometry method (LC-MS/MS) in order to quantify this novel drug … …American Journal of Animal and Veterinary Sciences, Vol. 13, Issue 2 · 24 May 2018 · 7,988 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Breeding Seasonality in Rusa Deer (Rusa timorensis) Stags via Serum Testosterone ProfilingWan Nor Fitri Wan Jaafar, Abd Wahid Haron, Rosnina Hj Yusoff et al.Breeding seasonality in mammals is influenced by the environmental changes and the endocrine response of the animals to that changes. Comprehension in breeding seasonality enables better reproductive management consequently maximizing the reproductive potential of the stags. Despite that, the study in breeding seasonality in Rusa deer (Rusa timorensis) is still scarce. Five healthy and matured stags were selected for this … …American Journal of Animal and Veterinary Sciences, Vol. 12, Issue 1 · 19 Mar 2017 · 8,608 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Lead in Human Teeth by Hydride Generation Atomic Absorption SpectrometryHassan T. AbdulsahibProblem statement: The determination of lead in human teeth at concentration levels of μg/ml is proposed using Hydride Generation Atomic Absorption Spectrometry (HG-AAS). To do this, 2% (wv) lanthanum chloride solution was employed as matrix modifying reagent to increase sensitivity and remove matrix interferences. Approach: About 100 μL of sample and 100 μL of 3.0% (m/v) NaBH4 are simultaneously injected … …American Journal of Environmental Sciences, Vol. 7, Issue 5 · 31 Oct 2011 · 7,133 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleSimultaneous Thermodynamic and Kinetic Parameters Determination Using Differential Scanning CalorimetryNader Frikha, Mohamed Bouroukba, Eric Schaer, Jean-Leon HouzelotProblem statement: The determination of reaction kinetics is of major importance, as for industrial reactors optimization as for environmental reasons or energy limitations. Although calorimetry is often used for the determination of thermodynamic parameters alone, the question that arises is: how can we apply the Differential Scanning Calorimetry for the determination of kinetic parameters. The objective of this study consists … …American Journal of Engineering and Applied Sciences, Vol. 4, Issue 1 · 12 Mar 2011 · 7,986 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Ibuprofen and Paracetamol in Binary Mixture Using Chemometric-Assisted Spectrophotometric MethodsWafaa S. HassanThree methods are presented for simultaneous determination of ibuprofen and paracetamol without previous separation. The first method depends on first derivative UV spectrophotometry, with zero-crossing measurement. The first derivative amplitudes at 230 and 290 nm were selected for the assay of ibuprofen and paracetamol, respectively. The second method depends on first derivative of the ratio-spectra by measurements of the amplitudes … …American Journal of Applied Sciences, Vol. 5, Issue 8 · 31 Aug 2008 · 8,199 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Metoprolol and Felodipine in Binary Mixture Using Chemometric-Assisted Spectrophotometric and High-Performance Liquid Chromatographic-UV MethodsHesham Salem, Ola M. AbdallahFour methods were developed for simultaneous determination of metoprolol and felodipine without previous separation. In the first method both drugs were determined using first derivative UV spectrophotometry, with zero crossing measurement at 222 and 235 nm for metoprolol and felodipine, respectively. The second method depends on first derivative of the ratios spectra by measurements of the amplitudes at 250.1 nm … …American Journal of Applied Sciences, Vol. 4, Issue 9 · 30 Sep 2007 · 8,025 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleAtomic Absorption Spectrometric Determination of Certain Fluoroquinolones in Pharmaceutical Dosage Forms and in Biological FluidsH. Salem, W. Khater, L. FadaSimple, accurate, sensitive and selective methods are described for the quantitative determination of ten fluoroquinolones (amifloxacin, ciprofloxacin hydrochloride, difloxacin hydrochloride, enoxacin, enrofloxacin, lomefloxacin hydrochloride, levofloxacin, norfloxacin, ofloxacin and pefloxacin mesylate). The methods are based on precipitation of the ion associates formed from the reaction of the cited drugs with silver nitrate, copper acetate and ferric chloride. The formation and solubility … …American Journal of Pharmacology and Toxicology, Vol. 2, Issue 2 · 30 Jun 2007 · 7,419 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleDetermination of Diloxanide Furoate and Metronidazole in Binary Mixture Using First Derivative of the Ratio-Spectra and High-Performance Liquid Chromatography-UV MethodsNora H. Al-ShaalanTwo methods are presented for simultaneous determination of diloxanide furoate and metronidazole. The first method depends on first derivative of the ratio-spectra by measurements of the amplitudes at 242.5 and 285.5 nm for diloxanide furoate and 225.5 and 300 nm for metrinidazole. Calibration graphs were established for 2-100 μg mL-1 for diloxanide furoate and 1-50 μg mL-1 for metronidazole. In … …American Journal of Applied Sciences, Vol. 4, Issue 2 · 28 Feb 2007 · 7,713 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleA New Spectrophotometric Method for Determination of Iron in Herbs, Spices and Beans with 2,6-Diacetylprydine Dioxime and 2-Acetylpyridine MonoximeZ. R. Komy, E. A. Abu-Gharib, A. DesokyThe reaction of iron (II) with 2, 6-diacetylprydine dioxime (H2dapd) and 2-acetylprydine monoxime (Hapm) in 10% and 60% v/v ethanol-water solution at pH 2.5 and 7.5, respectively, were studied using direct and first derivative spectrophotometry. Fe (III) is reduced by H2dapd and gives iron (II) complex. A simple, rapid, selective and sensitive method for the determination of Fe (II), Fe … …American Journal of Applied Sciences, Vol. 2, Issue 4 · 30 Apr 2005 · 6,960 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleSpectrofluorimetric, Atomic Absorption Spectrometric and Spectrophotometric Determination of Some FluoroquinolonesHesham SalemSimple, accurate, sensitive and selective spectrofluorimetric, atomic absorption spectrometric and spectrophotometric methods are described for the quantitative determination of ten fluoroquinolones (amifloxacin, ciprofloxacin hydrochloride, difloxacin hydrochloride, enoxacin, enrofloxacin, lomefloxacin hydrochloride, levofloxacin, norfloxacin, ofloxacin and pefloxacin mesylate). The first method was a spectrofluorimetric method in which samples of the studied drugs in 0.1 N H2SO4 showed native fluorescence at 450 nm … …American Journal of Applied Sciences, Vol. 2, Issue 3 · 31 Mar 2005 · 7,317 accessesView PDFCite