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86 articles for “x-ray diffraction”
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Research ArticleOpen accessPhrase in the titleX-Ray Diffraction and X-Ray Fluorescent Analyses of Prehistoric Pottery Shards from Ulu KelantanZuliskandar Ramli, Nik Hassan Shuhaimi Nik Abdul Rahman, Adnan Jusoh, Yunus SaumanProblem statement: X-Ray Diffraction (XRD) and X-Ray Fluorescent (XRF) were used in order to obtain mineralogical and elemental composition of seven pottery shards that have been unearthed during the excavation at Peraling Cave and Cha Cave in Ulu Kelantan, Malaysia. Approach: Peraling Cave and Cha Cave were prehistoric sites dating from 10, 000 BC which were inhabited by Hoabinhian people … …American Journal of Applied Sciences, Vol. 8, Issue 12 · 20 Oct 2011 · 7,751 accessesView PDFCite
Research ArticleOpen accessPhrase in the titleNew Mesogenic Schiff Base Esters with Polar Chloro Substituent: Synthesis, Thermotropic Properties and X-Ray Diffraction StudiesSie-Tiong Ha, Lay-Khoon Ong, Yasodha Sivasothy et al.Problem statement: Many studies have been conducted on the Schiff base’s alkyl and alkyloxy possessing terminal halogen substituent. However, the thermotropic properties of Schiff base’s ester (or alkanoyloxy) with chloro terminal group remained unstudied. Approach: Synthesis a series of new Schiff base ester possessing polar chloro group and investigate its mesomorphic properties. The title compounds were prepared via condensation and … …American Journal of Applied Sciences, Vol. 7, Issue 2 · 28 Feb 2010 · 12,956 accessesView PDFCite
Research ArticleOpen accessEvery word in the titleCrystal Structure of 2-(4-Hydroxy-3-Methoxyphenyl)-6- (4-Hydroxy-3-Methoxystyryl)-1-Methyl-2, 3-Dihydropyridine-4 (1H)-One by X-Ray Powder DiffractionBahjat A. Saeed, Kawkab Y. Saour, Rita S. Elias, Deng XiaodiProblem statement: The studied dihydropyridone was synthesized for the first time via the microwave assisted reaction of curcumin and methylamine and it is important to support the mechanism by the crystal structure. Approach: The crystal structure of the title compound was determined using high resolution x-ray diffraction. PowderSolve program was used to solve the structure while the refinement was done … …American Journal of Applied Sciences, Vol. 7, Issue 7 · 31 Jul 2010 · 7,160 accessesView PDFCite
Research ArticleOpen accessIn the keywordsFormation of Tl-1212 Phase in CR Substituted (Tl1-xCrx) Sr2CaCu2O7 SuperconductorRanjbar G.M., R. Abd-ShulorSuperconducting samples of (Tl1-xCrx) Sr2CaCu2O7 for x = 0.0-0.7 have been prepared by a solid state reaction technique at normal pressure using high purity elements. The powder X-ray diffraction patterns have been studied for samples. All samples showed the Tl-1212 as the major phase and Tl-1201 as the minor phase. The superconducting transition temperature Tc has been determined from the … …Physics International, Vol. 3, Issue 2 · 20 May 2013 · 6,694 accessesView PDFCite
Research ArticleOpen accessIn the keywordsStructural and Dielectrical Properties of Sterilized Human TeethMostafa Fawzy Eissa, Hassan Mohamed El-Shamy, Hassan Saad HanafyProblem statement: This study investigated the changes in crystallinity and dielectrical properties (conductivity) that could be demonstrated in extracted human teeth (enamel and dentin) subjected to γ-radiation at the sterilization dose (25 kGy). Approach: Twenty human third molar teeth were used in the study. Teeth were prepared so forty enamel and dentin samples were obtained. The samples were divided into … …Physics International, Vol. 3, Issue 1 · 20 Dec 2012 · 7,182 accessesView PDFCite
Research ArticleOpen accessIn the keywordsCompositional Analysis on Ancient Bricks from Candi Sungai Mas (Site 32/34), Bujang Valley, KedahZuliskandar Ramli, Nik Hassan Shuhaimi Nik Abd. Rahman, Adnan Jusoh, Mohd. Zobir HusseinProblem statement: The significance of Kampung Sungai Mas as an importance archaeology site in Lembah Bujang was revealed in the year 1979 when a cannel was built along Kampung Sungai Mas area. During the construction study of this cannel, thousands of ceramic pieces from India, Middle East, China, Southeast Asia and Europe was discovered, pieces of glasses from Middle East … …American Journal of Applied Sciences, Vol. 9, Issue 2 · 12 Dec 2011 · 9,839 accessesView PDFCite
Research ArticleOpen accessIn the keywordsInfluence of Triethanolamine on the Chemical Bath Deposited NiS Thin FilmsAnuar Kassim, Ho Soon Min, Tan Wee Tee, Ngai Chee FeiProblem statement: Recently, many scientists looking for new chalcogenide materials for the solar cell applications. Nowadays, silicon-based solar cell became dominant products in the market. Because of expensive silicon-based solar cells, scientists hope replaces it with cheaper chalcogenide materials. Approach: The binary chalcogenide materials were deposited onto microscope glass slide using simple chemical bath deposition method. Here, we study the … …American Journal of Applied Sciences, Vol. 8, Issue 4 · 18 Apr 2011 · 7,970 accessesView PDFCite
Research ArticleOpen accessIn the keywordsRelaxation of Residual Stress Part 2: Relaxation of Stage 2Omar Suliman Zaroog, Aidy Ali, B.B. Sahari, Rizal ZahariProblem statement: Compressive residual stress induced by surface treatment such as shot peening increased component’s fatigue life. However the initial induced residual stresses relax during component operating life and it is important to consider the relaxation in the design. Approach: In this study, a 2024-T351 aluminum alloy specimens were shot peened into three shot peening intensities condition to induce compressive … …American Journal of Engineering and Applied Sciences, Vol. 2, Issue 4 · 31 Dec 2009 · 7,997 accessesView PDFCite
Research ArticleOpen accessIn the keywordsSynthesis and Characterization of Silver/Clay/Chitosan Bionanocomposites by UV-Irradiation MethodMansor Bin Ahmad, Kamyar Shameli, Majid Darroudi et al.Problem statement: Silver/Montmorillonite/Chitosan Bionanocomposites (Ag/MMT/Cts BNCs) have been synthesized by UV-irradiation reduction method in the absence of any reducing agent or heat treatment which is used to antibacterial application and medical devices. Approach: MMT, Chitosan and AgNO3 were used as a solid support, stabilizer and silver precursor, respectively. The properties of Ag/MMT/Cts BNCs were studied as a function of UV-irradiation … …American Journal of Applied Sciences, Vol. 6, Issue 12 · 31 Dec 2009 · 8,815 accessesView PDFCite
Research ArticleOpen accessIn the keywordsSynthesis and Characterization of Silver/Clay Nanocomposites by Chemical Reduction MethodMansor Bin Ahmad, Kamyar Shameli, Majid Darroudi et al.Problem statement: Silver Nanoparticles (Ag-NPs) have been synthesized by using chemical reduction method into the interlayer space of a Montmorillonite (MMT) as a solid support which is used to antibacterial application and polymer nanocomposites for fabrication of medical devices. Approach: AgNO3 and NaBH4 were used as a silver precursor and reducing agent, respectively. The properties of Ag/MMT nanocomposites were studied … …American Journal of Applied Sciences, Vol. 6, Issue 11 · 30 Nov 2009 · 8,169 accessesView PDFCite