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Research ArticleOpen accessIn the keywordsGC-MS Analysis and PLS-DA Validation of the Trimethyl Silyl-Derivatization TechniquesKamalrul Azlan Azizan, Syarul Nataqain Baharum, Habtom W. Ressom, Normah Mohd. NoorProblem statement: Comparison and validation analysis of the conventional and power-adjusted Microwave-Assisted (MA) techniques of TMS derivatization using Gas Chromatography-Mass Spectrometry (GC-MS) and Multivariate Analysis (MVA) of Partial Least Squares Analysis (PLS-DA). Further improvement of the conventional technique using vigorous shaking was tested and analyzed. Approach: Cross-validation and response permutation test of PLS-DA and S-plot of Orthogonal Partial Least Squares … …American Journal of Applied Sciences, Vol. 9, Issue 7 · 4 Jun 2012 · 10,320 accessesView PDF Cite

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