148 results for “spectroscopy”

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Research ArticleOpen accessIn the abstractStability of Neodymium(III) Complexes of 4-Hydroxycoumarins with Anticoagulant ActivityIrena Kostova, Irina NikolovaComplexes of neodymium(III) with 4-hydroxy-3-(3-oxo-1-phenylbutyl)-2H-1-benzopyran-2-one, 4-hydroxy-3-[1-(4-chlorophenyl)-3-oxobutyl]-2H-1-benzopyran-2-one and 4-hydroxy-3-[1-(4-nitrophenyl)-3-oxobutyl]-2H-1-benzopyran-2-one were synthesized by mixing of water solutions of neodymium(III) nitrate and the respective ligands, in amounts equal to metal: ligand molar ratio of 1: 3. The complexes were characterized and identified by elemental analysis, conductivity, IR and 1H NMR spectral data. DTA and TGA have been applied to confirm the compositions of … …American Journal of Pharmacology and Toxicology, Vol. 1, Issue 2 · 30 Jun 2006 · 7,554 accessesView PDF Cite

Research ArticleOpen accessIn the abstractStatic and Dynamic Mechanical Behavior of Hydroxyapatite-Polyacrylic Acid Composites Under Simulated Body FluidKalpana S. Katti, Phanikumar Turlapati, Devendra Verma et al.In this work, we have investigated mechanical response of hydroxyapatite/polyacrylic composites under dry, wet and simulated body fluid conditions. Hydroxyapatite (HAP) is mineralized under two conditions; one, in presence of polyacrylic acid (in situ HAP), second, in absence of polyacrylic acid (ex situ HAP). Further, in situ and ex situ HAP are mixed with polyacrylic acid to make HAP/PAAc composites. … …American Journal of Biochemistry and Biotechnology, Vol. 2, Issue 2 · 30 Jun 2006 · 7,395 accessesView PDF Cite

Research ArticleOpen accessIn the abstractCharacterization of Chitosan-poly (Ethylene Oxide) Blends as Haemodialysis MembraneN. F. Mohd Nasir, N. Mohd Zain, M. G. Raha, N. A. KadriBlend membranes of chitosan and poly (ethylene oxide) with different molecular weights of 100,000 and 600,000 were prepared by the solution cast technique. The Chitosan-PEO blend membranes were produced to study their water adsorptions capacity and characteristics of the haemodialysis membrane application. An increase in the water adsorption capacity of chitosan-PEO blend membranes compared to the pure chitosan was due … …American Journal of Applied Sciences, Vol. 2, Issue 12 · 31 Dec 2005 · 8,426 accessesView PDF Cite

Research ArticleOpen accessIn the abstractThe Effects of Crosslinker and Monomer to the Polymerization of Polymethacrylamide Gel Dosimeters by Direct and Indirect MethodsElias Saion, A. H. Shaari, M. Z.A. Rahman et al.Radiation-induced polymerization in Polymethacrylamide Gels (PMAAGs) potentially used for 3D dose verification in radiotherapy has been studied using both Raman spectroscopy and Nuclear Magnetic Resonance (NMR) method. The dosimeters are composed of aqueous Methacrylamide (MAA) monomer and N, N’ methyelene-bis-acrylamide (BIS) crosslinker at various concentrations from 2 to 6% (w/w) and gelatin at 6% (w/w). The dosimeters were irradiated to … …American Journal of Applied Sciences, Vol. 2, Issue 8 · 31 Aug 2005 · 7,168 accessesView PDF Cite

Research ArticleOpen accessIn the abstractWavelet Shrinkage in Noise Removal of Hyperspectral Remote Sensing DataHelmi Z.M. Shafri, Paul M. MatherIt is common in hyperspectral remote sensing studies to perform analysis based on derivative spectroscopy. However, this technique is particularly sensitive to noise in the data. Thus, noise removal is essential before any derivative analysis. Various methods of noise removal are described in the literature. A newly developed method based on the wavelet transform appears promising, though there is little … …American Journal of Applied Sciences, Vol. 2, Issue 7 · 31 Jul 2005 · 7,013 accessesView PDF Cite

Research ArticleOpen accessIn the abstractUse of Cross-linking to Assess Subunit Interaction of Recombinant Human Coproporphyrinogen OxidaseJason R. Stephenson, Nancy E. Thomas, Jon A. Friesen, Marjorie A. JonesTo provide further evidence for a dimeric form of coproporphyrinogen oxidase reported using the conventional hydrodynamic methods, bifunctional cross-linkers were incubated with purified, recombinant human coproporphyrinogen oxidase to determine subunit interaction in solution. The use of cross-linkers provides an effective way to demonstrate subunit association and allows for assessment of activity upon covalent cross-linking. Following incubation with selected cross-linkers, enzyme … …American Journal of Biochemistry and Biotechnology, Vol. 1, Issue 2 · 30 Jun 2005 · 6,594 accessesView PDF Cite

Research ArticleOpen accessIn the abstractPreparation and Characterization of Hybrid Organic-Inorganic Composite Material: Polymerization of m-Aminobenzoic Acid-Intercalated Into Zn/Al-Layered Double HydroxidesRasheed M.A.Q. JamhourLayered double hydroxides of aluminum and zinc (Zn/Al-LDH’s) were synthesized directly by hydrolysis at room temperature as reported elsewhere. After characterization, the material was reacted with m-aminobenzoat anion (m-NH2C6H4COO-) which undergoes polymerization in the interlayer space; resulting in the formation of a matrix with polymeric organic macromolecule. The resulting material along with the host LDH’s compound of Zn/Al-Cl was characterized … …American Journal of Applied Sciences, Vol. 2, Issue 6 · 30 Jun 2005 · 6,586 accessesView PDF Cite

Research ArticleOpen accessIn the abstractSpectrofluorimetric, Atomic Absorption Spectrometric and Spectrophotometric Determination of Some FluoroquinolonesHesham SalemSimple, accurate, sensitive and selective spectrofluorimetric, atomic absorption spectrometric and spectrophotometric methods are described for the quantitative determination of ten fluoroquinolones (amifloxacin, ciprofloxacin hydrochloride, difloxacin hydrochloride, enoxacin, enrofloxacin, lomefloxacin hydrochloride, levofloxacin, norfloxacin, ofloxacin and pefloxacin mesylate). The first method was a spectrofluorimetric method in which samples of the studied drugs in 0.1 N H2SO4 showed native fluorescence at 450 nm … …American Journal of Applied Sciences, Vol. 2, Issue 3 · 31 Mar 2005 · 7,317 accessesView PDF Cite